Crystallization and Solid-state Annealing Studies of Poly(ether-ester) Multiblock Copolymers, Volume 2University of Wisconsin--Madison, 1992 - 650 pages |
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1-D correlation function 180 Temperature AH J/gm amorphous layer amorphous regions annealing temperature Bragg's Law calculated Chem crystal populations crystalline regions crystallization on cooling crystallization process crystallization rate degree of crystallinity demixing discussed in Chapter DSC scan development dual endotherm behavior electron density enthalpy Equation experimental Fakirov following melting fraction Freshly Cooled glass transition temperature hard segment concentration heat capacity homopolymer increase indicated temperatures initial molded isothermal crystallization lamellar thickness Macromolecules material melt quenched copolymers melting behavior memory effects mixed phase molded sample morphology observed original crystallization temperature peak melting temperature phase separation Phys poly(ether poly(ether-ester Polym polyurethane predicted primary melting recrystallization room temperature S.L. Cooper SAXS long spacing SAXS patterns semicrystalline sequence length softer copolymers solid line solid-state annealing spacing contraction spherulite structure studies suggests temperature annealing endotherm temperature dependence temperature endotherm University of Wisconsin-Madison values Vonk