Volatile Partitioning Between Milk Fat and Aqueous Phases as Influenced by Temperature |
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Page 36
2 Preparation of injection standards Partitioning of volatiles was measured
relative to an injection standard by gas chromatography with mass selective
detection ( GS - MSD ) . Standard curves relative to an injection standard were
prepared to ...
2 Preparation of injection standards Partitioning of volatiles was measured
relative to an injection standard by gas chromatography with mass selective
detection ( GS - MSD ) . Standard curves relative to an injection standard were
prepared to ...
Page 50
1 Standard Curve A standard curve is used to determine solute concentration
based on the mass selective detector response of the solute and injection
standard . Sections 3 . 1 . 1 to 3 . 1 . 5 describe methods used to prepare
standard curves .
1 Standard Curve A standard curve is used to determine solute concentration
based on the mass selective detector response of the solute and injection
standard . Sections 3 . 1 . 1 to 3 . 1 . 5 describe methods used to prepare
standard curves .
Page 106
4 Gas chromatography method development Delivery of GC injection samples
onto a GC column lacks precision due to the sample size and losses in the inlet .
Use of a known concentration injection standard allows for correction to account
...
4 Gas chromatography method development Delivery of GC injection samples
onto a GC column lacks precision due to the sample size and losses in the inlet .
Use of a known concentration injection standard allows for correction to account
...
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1-butanol 1-heptanol 1-octanol and water 1-propanol according acetone achieved acid activity Additional alcohols allowed analysis anhydrous milk fat approximately aqueous phase associated calculated cheese chromatography compared comparison compounds concentration conducted constant containing correlation crystal curve decrease dependent determined Deviation difference diffusion dissolved effect emulsion energy enthalpy entropy equilibrium conditions et al ethanol experiments factor fat and water flavor development globule greater groups hydrophobic impact improve increase indicates influenced by temperature initially injection standard interactions less levels limited lipid liquid Log Kmw mass mean measured melting method milk fat minutes mixing models needed observed partition coefficient peak area physical polar prepared properties proteins ratio reactions reduced regression reported sample saturated separate slope solid fat content solubility solute solvent stirring suggest Table understanding values verify versus vial volatiles volume water partitioning