Volatile Partitioning Between Milk Fat and Aqueous Phases as Influenced by Temperature |
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Page 41
Samples for GC - MSD analysis were prepared by removing a 100 uL sample of
the water phase from the bottom of an inverted partition vial . The sample was
expelled into a 2 mL glass vial , also with a Teflon - fluorocarbon - resin / silicone
...
Samples for GC - MSD analysis were prepared by removing a 100 uL sample of
the water phase from the bottom of an inverted partition vial . The sample was
expelled into a 2 mL glass vial , also with a Teflon - fluorocarbon - resin / silicone
...
Page 59
The large sample size at 20°C allowed for a more precise evaluation of the ra mo
se e probability behind equilibrium conditions versus stirring time . The means of
samples S ve initially dissolved in water were compared to samples dissolved ...
The large sample size at 20°C allowed for a more precise evaluation of the ra mo
se e probability behind equilibrium conditions versus stirring time . The means of
samples S ve initially dissolved in water were compared to samples dissolved ...
Page 105
3 Independent sample comparison of means In order to establish a more
accurate sample variance , a pooled variance ( sp2 ) was utilized according to
the following formula : 62 _ ( n , - 1 ) s ? + ( n2 – 1 ) sz ? n , + n2 – 2 ( 6 . 3 ) The
standard ...
3 Independent sample comparison of means In order to establish a more
accurate sample variance , a pooled variance ( sp2 ) was utilized according to
the following formula : 62 _ ( n , - 1 ) s ? + ( n2 – 1 ) sz ? n , + n2 – 2 ( 6 . 3 ) The
standard ...
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1-butanol 1-heptanol 1-octanol and water 1-propanol according acetone achieved acid activity Additional alcohols allowed analysis anhydrous milk fat approximately aqueous phase associated calculated cheese chromatography compared comparison compounds concentration conducted constant containing correlation crystal curve decrease dependent determined Deviation difference diffusion dissolved effect emulsion energy enthalpy entropy equilibrium conditions et al ethanol experiments factor fat and water flavor development globule greater groups hydrophobic impact improve increase indicates influenced by temperature initially injection standard interactions less levels limited lipid liquid Log Kmw mass mean measured melting method milk fat minutes mixing models needed observed partition coefficient peak area physical polar prepared properties proteins ratio reactions reduced regression reported sample saturated separate slope solid fat content solubility solute solvent stirring suggest Table understanding values verify versus vial volatiles volume water partitioning