Characterization of Catalytic MaterialsCatalytic materials are essential to nearly every commercial and industrial chemical process in order to make reaction times faster and more efficient. Understanding the microstructure of such materials is essential to designing improved catalytic properties. This volume in the materials characterization series reviews the more common types characterization methods used for understanding surface and structural properties of most types of commercially used catalytic materials.
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From inside the book
Results 1-5 of 53
Page v
... X-ray Diffraction and Scattering Methods 27 Particle Sizes from Line-Broadening 27, Small-Angle X-ray Scattering 28 2.5 Electron Microscopy 29 2.6 2.7 2.8 X-ray Absorption Spectroscopy v Contents.
... X-ray Diffraction and Scattering Methods 27 Particle Sizes from Line-Broadening 27, Small-Angle X-ray Scattering 28 2.5 Electron Microscopy 29 2.6 2.7 2.8 X-ray Absorption Spectroscopy v Contents.
Page vii
... X - ray , Neutron , and Electron Diffraction 132 7.4 7.5 Identification of Zeolites 134 , Compositional and Phase Changes 135 , Structure Determination by Diffraction Techniques 137 High - Resolution Electron Microscopy 138 Solid State ...
... X - ray , Neutron , and Electron Diffraction 132 7.4 7.5 Identification of Zeolites 134 , Compositional and Phase Changes 135 , Structure Determination by Diffraction Techniques 137 High - Resolution Electron Microscopy 138 Solid State ...
Page viii
... X-ray Diffraction Pattern 152, Elemental Analysis 153, Electron Microscopy 154, Pore Structure by Adsorption–Desorption Techniques 155, Surface Acidity 158, 29Si and 27Al MAS- NMR 158, Pillared Clays As Catalysts 159 8.4 Summary 161 ...
... X-ray Diffraction Pattern 152, Elemental Analysis 153, Electron Microscopy 154, Pore Structure by Adsorption–Desorption Techniques 155, Surface Acidity 158, 29Si and 27Al MAS- NMR 158, Pillared Clays As Catalysts 159 8.4 Summary 161 ...
Page ix
... X-Ray Diffraction (XRD) 193 28 X-Ray Fluorescence (XRF) 194 29 X-Ray Photoelectron and Auger Electron Diffraction (XPD and AED) 195 30 X-Ray Photoelectron Spectroscopy (XPS) 196 Index 197 x Preface to the Reissue of the Materials ...
... X-Ray Diffraction (XRD) 193 28 X-Ray Fluorescence (XRF) 194 29 X-Ray Photoelectron and Auger Electron Diffraction (XPD and AED) 195 30 X-Ray Photoelectron Spectroscopy (XPS) 196 Index 197 x Preface to the Reissue of the Materials ...
Page 5
... X-ray fluorescence and neutron activation analysis are also widely used methods that have the advantage of not ... diffraction is a powerful method used in the determination of the bulk crystal- lographic structure of catalytic materials; it ...
... X-ray fluorescence and neutron activation analysis are also widely used methods that have the advantage of not ... diffraction is a powerful method used in the determination of the bulk crystal- lographic structure of catalytic materials; it ...
Contents
1 | |
17 | |
3 Bulk Metal Oxides | 47 |
4 Supported Metal Oxides | 69 |
5 Bulk Metal Sulfides | 89 |
6 Supported Metal Sulfides | 109 |
7 Zeolites and Molecular Sieves | 129 |
Methods of Preparation and Characterization | 149 |
LowEnergy Electron Diffraction LEED | 179 |
Mössbauer Spectroscopy | 180 |
Neutron Activation Analysis NAA | 181 |
Neutron Diffraction | 182 |
Physical and Chemical Adsorption for the Measurement of Solid Surface Areas | 183 |
Raman Spectroscopy | 184 |
Scanning Electron Microscopy SEM | 185 |
Scanning Transmission Electron Microscopy STEM | 186 |
Technique Summaries | 165 |
Auger Electron Spectroscopy AES | 167 |
Dynamic Secondary Ion Mass Spectrometry DSIMS | 168 |
Electron Energyloss Spectroscopy in the Transmission Electron Microscope EELS | 169 |
Electron Paramagnetic Resonance Electron Spin Resonance | 170 |
Electron Microprobe XRay Microanalysis EPMA | 171 |
EnergyDispersive XRay Spectroscopy EDS | 172 |
Extended XRay Absorption Fine Structure EXAFS | 173 |
Fourier Transform Infrared Spectroscopy FTIR | 174 |
High Resolution Electron Energy Loss Spectroscopy HREELS | 175 |
Inductively Coupled Plasma Mass Spectrometry ICPMS | 176 |
Inductively Coupled PlasmaOptical Emission Spectroscopy ICPOES | 177 |
Ion Scattering Spectroscopy ISS | 178 |
Scanning Tunneling Microscopy and Scanning Force Microscopy STM and SFM | 187 |
Solid State Nuclear Magnetic Resonance NMR | 188 |
Static Secondary Ion Mass Spectrometry Static SIMS | 189 |
Temperature Programmed Techniques | 190 |
Transmission Electron Microscopy TEM | 191 |
Ultraviolet Photoelectron Spectroscopy UPS | 192 |
XRay Diffraction XRD | 193 |
XRay Fluorescence XRF | 194 |
XRay Photoelectron and Auger Electron Diffraction XRD and AED | 195 |
XRay Photoelectron Spectroscopy XPS | 196 |
Index | 197 |
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Common terms and phrases
acid adsorbed adsorption alloys alumina aluminum analysis atoms beam bond bulk metal calcination Catal catalytic activity catalytic behavior catalytic materials cation Chem chemical chemical shifts chemisorption Chemistry cobalt coordination crystalline crystallites desorption determine electron microscopy elements energy EXAFS faujasites Figure function hydrogen hydrogenolysis I. E. Wachs interaction lattice layer measured metal catalysts metal oxide catalysts metal oxide overlayers metal oxide phases microporous Mo ions molecular sieves molecules molybdenum oxide monolayer coverage MoS2 Mössbauer Mössbauer spectroscopy neutron obtained oxide support oxygen particle peak photoelectron pillared clays pore powder preparation probe promoter R. R. Chianelli Raman Raman spectroscopy reaction reduced resolution ruthenium sample single crystal solid solution species spectra spectroscopy structure studies sulfides sulfur supported metal oxide surface area surface metal oxide synchrotron techniques temperature temperature-programmed thiophene tion transmission electron microscopy two-dimensional metal oxide X-ray absorption X-ray diffraction XANES zeolites