Characterization of Catalytic MaterialsCatalytic materials are essential to nearly every commercial and industrial chemical process in order to make reaction times faster and more efficient. Understanding the microstructure of such materials is essential to designing improved catalytic properties. This volume in the materials characterization series reviews the more common types characterization methods used for understanding surface and structural properties of most types of commercially used catalytic materials.
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Page xiii
These characterization methods have become our “eyes” and are indispensible
in the development of new catalytic materials. It is hard to conceive of a modern
heterogeneous catalysis activity, be it research or manufacturing, without the aid
...
These characterization methods have become our “eyes” and are indispensible
in the development of new catalytic materials. It is hard to conceive of a modern
heterogeneous catalysis activity, be it research or manufacturing, without the aid
...
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Contents
| 1 | |
| 17 | |
3 Bulk Metal Oxides | 47 |
4 Supported Metal Oxides | 69 |
5 Bulk Metal Sulfides | 89 |
6 Supported Metal Sulfides | 109 |
7 Zeolites and Molecular Sieves | 129 |
Methods of Preparation and Characterization | 149 |
LowEnergy Electron Diffraction LEED | 179 |
Mössbauer Spectroscopy | 180 |
Neutron Activation Analysis NAA | 181 |
Neutron Diffraction | 182 |
Physical and Chemical Adsorption for the Measurement of Solid Surface Areas | 183 |
Raman Spectroscopy | 184 |
Scanning Electron Microscopy SEM | 185 |
Scanning Transmission Electron Microscopy STEM | 186 |
Technique Summaries | 165 |
Auger Electron Spectroscopy AES | 167 |
Dynamic Secondary Ion Mass Spectrometry DSIMS | 168 |
Electron Energyloss Spectroscopy in the Transmission Electron Microscope EELS | 169 |
Electron Paramagnetic Resonance Electron Spin Resonance | 170 |
Electron Microprobe XRay Microanalysis EPMA | 171 |
EnergyDispersive XRay Spectroscopy EDS | 172 |
Extended XRay Absorption Fine Structure EXAFS | 173 |
Fourier Transform Infrared Spectroscopy FTIR | 174 |
High Resolution Electron Energy Loss Spectroscopy HREELS | 175 |
Inductively Coupled Plasma Mass Spectrometry ICPMS | 176 |
Inductively Coupled PlasmaOptical Emission Spectroscopy ICPOES | 177 |
Ion Scattering Spectroscopy ISS | 178 |
Scanning Tunneling Microscopy and Scanning Force Microscopy STM and SFM | 187 |
Solid State Nuclear Magnetic Resonance NMR | 188 |
Static Secondary Ion Mass Spectrometry Static SIMS | 189 |
Temperature Programmed Techniques | 190 |
Transmission Electron Microscopy TEM | 191 |
Ultraviolet Photoelectron Spectroscopy UPS | 192 |
XRay Diffraction XRD | 193 |
XRay Fluorescence XRF | 194 |
XRay Photoelectron and Auger Electron Diffraction XRD and AED | 195 |
XRay Photoelectron Spectroscopy XPS | 196 |
Index | 197 |
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Common terms and phrases
acid adsorbed adsorption alloys alumina aluminum analysis atoms Auger beam bond bulk metal calcination Catal catalytic activity catalytic behavior catalytic materials cation Chem chemical chemical shifts chemisorption Chemistry Co–Mo–S cobalt coordination correlation crystalline crystallites desorption determine electron microscopy elements EXAFS Figure function hydrogen hydrogenolysis hydrotreating catalysts interaction layer measured metal catalysts metal oxide catalysts metal oxide overlayers metal oxide phases microporous Mo ions molecular sieves molecules molybdenum oxide monolayer coverage MoS2 Mössbauer Mössbauer effect Mössbauer spectroscopy neutron obtained oxide support oxygen particle peak photoelectron pillared clays pore powder preparation probe promoter Raman spectroscopy reaction reduced resolution ruthenium sample single crystal solid solution species spectra structure studies sulfides sulfur supported metal oxide surface area surface composition surface metal oxide synchrotron techniques temperature temperature-programmed thiophene tion transmission electron microscopy two-dimensional metal oxide X-ray absorption X-ray diffraction XANES zeolites
Bibliographic information
| Title | Characterization of Catalytic Materials Materials characterization series |
| Author | Israel E. Wachs |
| Editor | Israel E. Wachs |
| Edition | reprint, reissue, revised |
| Publisher | Momentum Press, 2010 |
| ISBN | 1606501844, 9781606501849 |
| Length | 202 pages |
| Subjects | › › Science / Chemistry / General Technology & Engineering / Chemical & Biochemical Technology & Engineering / Materials Science / General Technology & Engineering / Metallurgy |
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