Characterization of Catalytic MaterialsCatalytic materials are essential to nearly every commercial and industrial chemical process in order to make reaction times faster and more efficient. Understanding the microstructure of such materials is essential to designing improved catalytic properties. This volume in the materials characterization series reviews the more common types characterization methods used for understanding surface and structural properties of most types of commercially used catalytic materials.
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From inside the book
Results 1-5 of 18
Page vii
... Neutron, and Electron Diffraction 132 Identification of Zeolites 134, Compositional and Phase Changes 135, Structure Determination by Diffraction Techniques 137 7.4 High-Resolution Electron Microscopy 138 7.5 Solid State NMR ...
... Neutron, and Electron Diffraction 132 Identification of Zeolites 134, Compositional and Phase Changes 135, Structure Determination by Diffraction Techniques 137 7.4 High-Resolution Electron Microscopy 138 7.5 Solid State NMR ...
Page viii
... Emission Spectroscopy (ICP-OES) 177 12 Ion Scattering Spectroscopy (ISS) 178 13 Low-Energy Electron Diffraction (LEED) 179 14 Mössbauer Spectroscopy 180 15 Neutron Activation Analysis (NAA) 181 16 Neutron Diffraction 182 viii Contents.
... Emission Spectroscopy (ICP-OES) 177 12 Ion Scattering Spectroscopy (ISS) 178 13 Low-Energy Electron Diffraction (LEED) 179 14 Mössbauer Spectroscopy 180 15 Neutron Activation Analysis (NAA) 181 16 Neutron Diffraction 182 viii Contents.
Page ix
Israel E. Wachs. 15 Neutron Activation Analysis (NAA) 181 16 Neutron Diffraction 182 17 Physical and Chemical Adsorption for the Measurement of Solid State Areas 183 18 Raman Spectroscopy 184 19 Scanning Electron Microscopy (SEM) 185 20 ...
Israel E. Wachs. 15 Neutron Activation Analysis (NAA) 181 16 Neutron Diffraction 182 17 Physical and Chemical Adsorption for the Measurement of Solid State Areas 183 18 Raman Spectroscopy 184 19 Scanning Electron Microscopy (SEM) 185 20 ...
Page 5
... neutron activation analysis are also widely used methods that have the advantage of not requiring the dissolution of the metal or of the alloy. X-ray fluorescence analysis is most sensitive for elements with high atomic weight. Bulk ...
... neutron activation analysis are also widely used methods that have the advantage of not requiring the dissolution of the metal or of the alloy. X-ray fluorescence analysis is most sensitive for elements with high atomic weight. Bulk ...
Page 14
... neutron activation analysis. X-ray diffraction has been a powerful and accurate method for the determination of bulk crystallographic structures, but recent developments in high-resolution and analytical electron microscopy, which allow ...
... neutron activation analysis. X-ray diffraction has been a powerful and accurate method for the determination of bulk crystallographic structures, but recent developments in high-resolution and analytical electron microscopy, which allow ...
Contents
1 | |
17 | |
3 Bulk Metal Oxides | 47 |
4 Supported Metal Oxides | 69 |
5 Bulk Metal Sulfides | 89 |
6 Supported Metal Sulfides | 109 |
7 Zeolites and Molecular Sieves | 129 |
Methods of Preparation and Characterization | 149 |
LowEnergy Electron Diffraction LEED | 179 |
Mössbauer Spectroscopy | 180 |
Neutron Activation Analysis NAA | 181 |
Neutron Diffraction | 182 |
Physical and Chemical Adsorption for the Measurement of Solid Surface Areas | 183 |
Raman Spectroscopy | 184 |
Scanning Electron Microscopy SEM | 185 |
Scanning Transmission Electron Microscopy STEM | 186 |
Technique Summaries | 165 |
Auger Electron Spectroscopy AES | 167 |
Dynamic Secondary Ion Mass Spectrometry DSIMS | 168 |
Electron Energyloss Spectroscopy in the Transmission Electron Microscope EELS | 169 |
Electron Paramagnetic Resonance Electron Spin Resonance | 170 |
Electron Microprobe XRay Microanalysis EPMA | 171 |
EnergyDispersive XRay Spectroscopy EDS | 172 |
Extended XRay Absorption Fine Structure EXAFS | 173 |
Fourier Transform Infrared Spectroscopy FTIR | 174 |
High Resolution Electron Energy Loss Spectroscopy HREELS | 175 |
Inductively Coupled Plasma Mass Spectrometry ICPMS | 176 |
Inductively Coupled PlasmaOptical Emission Spectroscopy ICPOES | 177 |
Ion Scattering Spectroscopy ISS | 178 |
Scanning Tunneling Microscopy and Scanning Force Microscopy STM and SFM | 187 |
Solid State Nuclear Magnetic Resonance NMR | 188 |
Static Secondary Ion Mass Spectrometry Static SIMS | 189 |
Temperature Programmed Techniques | 190 |
Transmission Electron Microscopy TEM | 191 |
Ultraviolet Photoelectron Spectroscopy UPS | 192 |
XRay Diffraction XRD | 193 |
XRay Fluorescence XRF | 194 |
XRay Photoelectron and Auger Electron Diffraction XRD and AED | 195 |
XRay Photoelectron Spectroscopy XPS | 196 |
Index | 197 |
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Common terms and phrases
acid activity adsorbed adsorption alloys American Chemical Society amount analysis application atoms beam bismuth bond bulk calcination Catal cation changes characterization Chem chemical chemisorption Chemistry cobalt composition contain coordination correlation crystal crystalline depends detected determine diffraction distribution edge effect electron electron microscopy elements energy example Figure function hydrogen identification important indicates intensity interaction ions layer materials measured metal oxide method molecular sieves molecules molybdenum MoS2 Mössbauer observed obtained occur oxide catalysts oxygen particle peak phase pillared clays pore possible powder preparation present probe produce promoter properties Raman Raman spectroscopy range reaction reduced Reference relationship requires resolution sample scattering sensitive shows single solid solution species spectra spectroscopy structure studies sulfides supported metal oxide surface area techniques temperature tion typically usually volume X-ray X-ray diffraction zeolites