Characterization of Catalytic MaterialsCatalytic materials are essential to nearly every commercial and industrial chemical process in order to make reaction times faster and more efficient. Understanding the microstructure of such materials is essential to designing improved catalytic properties. This volume in the materials characterization series reviews the more common types characterization methods used for understanding surface and structural properties of most types of commercially used catalytic materials.
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From inside the book
Results 1-5 of 82
Page vii
... Techniques 97 Structure - Function Relationships 100 5.5 Importance of the Electronic Structure 100 , Structure 102 , Effect of the Sulfur Vacancies Effect of the Crystallographic 104 5.6 Summary 105 SUPPORTED METAL SULFIDES 6.1 ...
... Techniques 97 Structure - Function Relationships 100 5.5 Importance of the Electronic Structure 100 , Structure 102 , Effect of the Sulfur Vacancies Effect of the Crystallographic 104 5.6 Summary 105 SUPPORTED METAL SULFIDES 6.1 ...
Page viii
... Techniques 155, Surface Acidity 158, 29Si and 27Al MAS- NMR 158, Pillared Clays As Catalysts 159 8.4 Summary 161 APPENDIXES: TECHNIQUES SUMMARIES 1 Auger Electron Spectroscopy (AES) 167 2 Dynamic Secondary Ion Mass Spectrometry (D-SIMS) ...
... Techniques 155, Surface Acidity 158, 29Si and 27Al MAS- NMR 158, Pillared Clays As Catalysts 159 8.4 Summary 161 APPENDIXES: TECHNIQUES SUMMARIES 1 Auger Electron Spectroscopy (AES) 167 2 Dynamic Secondary Ion Mass Spectrometry (D-SIMS) ...
Page ix
... Techniques 190 189 26 Ultraviolet Photoelectron Spectroscopy (UPS) 192 27 X-Ray Diffraction (XRD) 193 28 X-Ray Fluorescence (XRF) 194 29 X-Ray Photoelectron and Auger Electron Diffraction (XPD and AED) 195 30 X-Ray Photoelectron ...
... Techniques 190 189 26 Ultraviolet Photoelectron Spectroscopy (UPS) 192 27 X-Ray Diffraction (XRD) 193 28 X-Ray Fluorescence (XRF) 194 29 X-Ray Photoelectron and Auger Electron Diffraction (XPD and AED) 195 30 X-Ray Photoelectron ...
Page xi
... technique, introductory summaries to group- ings of related techniques, a complete glossary of acronyms, and a tabular compari- son of the major features of all 50 techniques. The 10 volumes in the Series on characterization of ...
... technique, introductory summaries to group- ings of related techniques, a complete glossary of acronyms, and a tabular compari- son of the major features of all 50 techniques. The 10 volumes in the Series on characterization of ...
Page xii
... techniques needed to characterize both materials and properties over the wide range involved, was put together by 11 individual experts, split between academia, oil com- pany research and engineering laboratories, and a national ...
... techniques needed to characterize both materials and properties over the wide range involved, was put together by 11 individual experts, split between academia, oil com- pany research and engineering laboratories, and a national ...
Contents
1 | |
17 | |
3 Bulk Metal Oxides | 47 |
4 Supported Metal Oxides | 69 |
5 Bulk Metal Sulfides | 89 |
6 Supported Metal Sulfides | 109 |
7 Zeolites and Molecular Sieves | 129 |
Methods of Preparation and Characterization | 149 |
LowEnergy Electron Diffraction LEED | 179 |
Mössbauer Spectroscopy | 180 |
Neutron Activation Analysis NAA | 181 |
Neutron Diffraction | 182 |
Physical and Chemical Adsorption for the Measurement of Solid Surface Areas | 183 |
Raman Spectroscopy | 184 |
Scanning Electron Microscopy SEM | 185 |
Scanning Transmission Electron Microscopy STEM | 186 |
Technique Summaries | 165 |
Auger Electron Spectroscopy AES | 167 |
Dynamic Secondary Ion Mass Spectrometry DSIMS | 168 |
Electron Energyloss Spectroscopy in the Transmission Electron Microscope EELS | 169 |
Electron Paramagnetic Resonance Electron Spin Resonance | 170 |
Electron Microprobe XRay Microanalysis EPMA | 171 |
EnergyDispersive XRay Spectroscopy EDS | 172 |
Extended XRay Absorption Fine Structure EXAFS | 173 |
Fourier Transform Infrared Spectroscopy FTIR | 174 |
High Resolution Electron Energy Loss Spectroscopy HREELS | 175 |
Inductively Coupled Plasma Mass Spectrometry ICPMS | 176 |
Inductively Coupled PlasmaOptical Emission Spectroscopy ICPOES | 177 |
Ion Scattering Spectroscopy ISS | 178 |
Scanning Tunneling Microscopy and Scanning Force Microscopy STM and SFM | 187 |
Solid State Nuclear Magnetic Resonance NMR | 188 |
Static Secondary Ion Mass Spectrometry Static SIMS | 189 |
Temperature Programmed Techniques | 190 |
Transmission Electron Microscopy TEM | 191 |
Ultraviolet Photoelectron Spectroscopy UPS | 192 |
XRay Diffraction XRD | 193 |
XRay Fluorescence XRF | 194 |
XRay Photoelectron and Auger Electron Diffraction XRD and AED | 195 |
XRay Photoelectron Spectroscopy XPS | 196 |
Index | 197 |
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Common terms and phrases
acid adsorbed adsorption alloys alumina aluminum analysis atoms beam bond bulk metal calcination Catal catalytic activity catalytic behavior catalytic materials cation Chem chemical chemical shifts chemisorption Chemistry cobalt coordination crystalline crystallites desorption determine electron microscopy elements energy EXAFS faujasites Figure function hydrogen hydrogenolysis I. E. Wachs interaction lattice layer measured metal catalysts metal oxide catalysts metal oxide overlayers metal oxide phases microporous Mo ions molecular sieves molecules molybdenum oxide monolayer coverage MoS2 Mössbauer Mössbauer spectroscopy neutron obtained oxide support oxygen particle peak photoelectron pillared clays pore powder preparation probe promoter R. R. Chianelli Raman Raman spectroscopy reaction reduced resolution ruthenium sample single crystal solid solution species spectra spectroscopy structure studies sulfides sulfur supported metal oxide surface area surface metal oxide synchrotron techniques temperature temperature-programmed thiophene tion transmission electron microscopy two-dimensional metal oxide X-ray absorption X-ray diffraction XANES zeolites