X-Ray Diffraction: A Practical ApproachIn this, the only book available to combine both theoretical and practical aspects of x-ray diffraction, the authors emphasize a "hands on" approach through experiments and examples based on actual laboratory data. Part I presents the basics of x-ray diffraction and explains its use in obtaining structural and chemical information. In Part II, eight experimental modules enable the students to gain an appreciation for what information can be obtained by x-ray diffraction and how to interpret it. Examples from all classes of materials -- metals, ceramics, semiconductors, and polymers -- are included. Diffraction patterns and Bragg angles are provided for students without diffractometers. 192 illustrations. |
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... crystals in 1912 ( by Max von Laue ) and its immediate application to structure determination in 1913 ( by W. L. Bragg and his father W. H. Bragg ) paved the way for successful utilization of this technique to determine crystal structures ...
... crystals in 1912 ( by Max von Laue ) and its immediate application to structure determination in 1913 ( by W. L. Bragg and his father W. H. Bragg ) paved the way for successful utilization of this technique to determine crystal structures ...
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... crystal structures adopted by materials . Additionally , the phenomena of diffraction of x - rays by crystalline materials , concepts of structure factor , and selection rules for the observance ( or absence ) of reflections are ...
... crystal structures adopted by materials . Additionally , the phenomena of diffraction of x - rays by crystalline materials , concepts of structure factor , and selection rules for the observance ( or absence ) of reflections are ...
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... Lattice Point 3 5 14 18 21 232 24 27 27 31 36 2.4.4 . More than Two Atoms per Lattice Point . 40 · 2.5 . Notation for Crystal Structures 41 2.6 . Miller Indices 43 2.7 . Diffraction from Crystalline Materials— Bragg's Law 2.8 . The ...
... Lattice Point 3 5 14 18 21 232 24 27 27 31 36 2.4.4 . More than Two Atoms per Lattice Point . 40 · 2.5 . Notation for Crystal Structures 41 2.6 . Miller Indices 43 2.7 . Diffraction from Crystalline Materials— Bragg's Law 2.8 . The ...
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... Crystal Structure Determination . I : Cubic Structures 97 Module 2. Crystal Structure Determination . II : Hexagonal Structures 125 Module 3. Precise Lattice Parameter Measurements . Module 4. Phase Diagram Determination • • Module 5 ...
... Crystal Structure Determination . I : Cubic Structures 97 Module 2. Crystal Structure Determination . II : Hexagonal Structures 125 Module 3. Precise Lattice Parameter Measurements . Module 4. Phase Diagram Determination • • Module 5 ...
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... Structure Factor Calculations . Appendix 5. Mass Absorption Coefficients μ / p ( cm / g ) and Densities p ( g / cm3 ) ... Crystal Structures and Lattice Parameters of Some Selected Materials Bibliography . • Index · 262 263 265 271 Part I ...
... Structure Factor Calculations . Appendix 5. Mass Absorption Coefficients μ / p ( cm / g ) and Densities p ( g / cm3 ) ... Crystal Structures and Lattice Parameters of Some Selected Materials Bibliography . • Index · 262 263 265 271 Part I ...
Contents
3 | |
21 | |
Practical Aspects of XRay Diffraction | 63 |
Cubic Structures | 94 |
Hexagonal Structures | 125 |
Precise Lattice Parameter Measurements | 153 |
Phase Diagram Determination | 167 |
Quantitative Analysis of Powder Mixtures | 223 |
Identification of an Unknown Specimen | 237 |
Appendixes | 251 |
Atomic and lonic Scattering Factors of Some Selected | 255 |
Physical Constants and Conversion Factors | 261 |
Index | 271 |
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Common terms and phrases
20 values absorption alloy aluminum amplitude ångstrom atomic scattering factor atoms per cell atoms per unit body-centered cubic Bragg angle Bragg's law Bravais lattice broadening close-packed components composition copper cos² crystal structure crystal systems crystallite CsCl cubic Bravais lattice detector determine diamond cubic diamond cubic structure diffracted beam electron energy equation example Experimental Module face-centered cubic face-centered cubic Bravais face-centering translations fcc structure grain hexagonal hkl a nm integrated intensity lattice parameter lattice parameter(s lattice point lattice strain metal Miller indices mixture NaCl structure obtained orthorhombic phase diagram point lattice polycrystalline powder quantum number radiation relative intensities shell shown in Fig silicon simple cubic sin² sin² 0 sin² sin² 0 values slits solid solution spacing structure factor Table Theta FIG Titanium unit cell unknown specimen wavelength x-ray diffraction pattern x-ray photon zinc blende