Solid State Behavior of Linear Polyesters and Polyamides |
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Page 104
SAXS measurements are very useful in following the development of
microstructure . ... and amorphous domains ) have dimensions of units or tens of
nanometers and it is precisely in this range that SAXS provides a microstructural
probe .
SAXS measurements are very useful in following the development of
microstructure . ... and amorphous domains ) have dimensions of units or tens of
nanometers and it is precisely in this range that SAXS provides a microstructural
probe .
Page 115
SAXS , often combined with WAXS , has been used in postmortem investigations
, to study details of microstructure at the 100 A level . A typical SAXS pattern for
PET crystallized under substantial strain consists of four streaks , as shown in ...
SAXS , often combined with WAXS , has been used in postmortem investigations
, to study details of microstructure at the 100 A level . A typical SAXS pattern for
PET crystallized under substantial strain consists of four streaks , as shown in ...
Page 143
Preliminary SAXS data were obtained with a rotating anode generator employing
a two - pinhole collimating system with 20 cm ... More precise SAXS data were
obtained using a monochromatic line focus system that allowed only copper Kai ...
Preliminary SAXS data were obtained with a rotating anode generator employing
a two - pinhole collimating system with 20 cm ... More precise SAXS data were
obtained using a monochromatic line focus system that allowed only copper Kai ...
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achieved acid additional amorphous annealing Appl applied aspect average behavior block bonding changes Chem chemical composites conclusion constant crack crystallinity crystallization curves decreases deformation density depends determined diameter diffusion direction distribution domains draw ratio drawn effect element energy Equation experiments extrusion factor fatigue fiber Figure fracture fracture toughness function given groups growth healing heat higher important increasing indicated initial length linear load lower material matrix maximum measurements mechanical melt method microfibrils microstructure modulus molded molecular weight molecules nylon nylon 66 observed obtained occurs orientation peak phase Phys polyamides polycondensation polyesters Polymer Sci polymerization properties range reaction regions reported Reprinted from Ref respectively samples SAXS scattering shows solid solid state polycondensation solid-state specimen speed stage strain strength stress structure studied Table temperature tensile units values yield