Solid State Behavior of Linear Polyesters and Polyamides |
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Page 89
This last method is employed in heat of fusion measurements of DC . There are
substantial problems connected with the use of any of these methods . Perhaps
the most important problem is that the properties of the individual phases are not
...
This last method is employed in heat of fusion measurements of DC . There are
substantial problems connected with the use of any of these methods . Perhaps
the most important problem is that the properties of the individual phases are not
...
Page 139
Dynamic Mechanical Measurement . Measurements of dynamic tensile modulus
E ' and mechanical loss factor tan & were made using a Vibron - type dynamic
viscoelastometer . Temperature plots were obtained by increasing the specimen
...
Dynamic Mechanical Measurement . Measurements of dynamic tensile modulus
E ' and mechanical loss factor tan & were made using a Vibron - type dynamic
viscoelastometer . Temperature plots were obtained by increasing the specimen
...
Page 185
measurements were made of the filament temperature and diameter at each
sleeve . The filament temperature was also measured by the contact null - point
device , and the filament diameter was measured by close - up photography .
measurements were made of the filament temperature and diameter at each
sleeve . The filament temperature was also measured by the contact null - point
device , and the filament diameter was measured by close - up photography .
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achieved acid additional amorphous annealing Appl applied aspect average behavior block bonding changes Chem chemical composites conclusion constant crack crystallinity crystallization curves decreases deformation density depends determined diameter diffusion direction distribution domains draw ratio drawn effect element energy Equation experiments extrusion factor fatigue fiber Figure fracture fracture toughness function given groups growth healing heat higher important increasing indicated initial length linear load lower material matrix maximum measurements mechanical melt method microfibrils microstructure modulus molded molecular weight molecules nylon nylon 66 observed obtained occurs orientation peak phase Phys polyamides polycondensation polyesters Polymer Sci polymerization properties range reaction regions reported Reprinted from Ref respectively samples SAXS scattering shows solid solid state polycondensation solid-state specimen speed stage strain strength stress structure studied Table temperature tensile units values yield