Sample Preparation Techniques in Analytical ChemistrySomenath Mitra The importance of accurate sample preparation techniques cannot be overstated--meticulous sample preparation is essential. Often overlooked, it is the midway point where the analytes from the sample matrix are transformed so they are suitable for analysis. Even the best analytical techniques cannot rectify problems generated by sloppy sample pretreatment. Devoted entirely to teaching and reinforcing these necessary pretreatment steps, Sample Preparation Techniques in Analytical Chemistry addresses diverse aspects of this important measurement step. These include: * State-of-the-art extraction techniques for organic and inorganic analytes * Sample preparation in biological measurements * Sample pretreatment in microscopy * Surface enhancement as a sample preparation tool in Raman and IR spectroscopy * Sample concentration and clean-up methods * Quality control steps Designed to serve as a text in an undergraduate or graduate level curriculum, Sample Preparation Techniques in Analytical Chemistry also provides an invaluable reference tool for analytical chemists in the chemical, biological, pharmaceutical, environmental, and materials sciences. |
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Page viii
... EXTRACTION AND ENRICHMENT IN SAMPLE PREPARATION PRINCIPLES OF EXTRACTION AND THE EXTRACTION OF SEMIVOLATILE ORGANICS ... Solid Extraction 2.3.1. Sorption Solid-Phase Extraction 2.4.1. Sorbents in SPE 2.4.2. Sorbent Selection 2.4.3 ...
... EXTRACTION AND ENRICHMENT IN SAMPLE PREPARATION PRINCIPLES OF EXTRACTION AND THE EXTRACTION OF SEMIVOLATILE ORGANICS ... Solid Extraction 2.3.1. Sorption Solid-Phase Extraction 2.4.1. Sorbents in SPE 2.4.2. Sorbent Selection 2.4.3 ...
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... SPE 2.5. Solid-Phase Microextraction 2.5.1. Sorbents 2.5.2. Sorbent Selection 2.5.3. Methodology 2.5.4. Recent Advances in Techniques 2.6. Stir Bar Sorptive Extraction 2.6.1. Sorbent and Analyte Recovery 2.6.2. Methodology 2.6.3. Recent ...
... SPE 2.5. Solid-Phase Microextraction 2.5.1. Sorbents 2.5.2. Sorbent Selection 2.5.3. Methodology 2.5.4. Recent Advances in Techniques 2.6. Stir Bar Sorptive Extraction 2.6.1. Sorbent and Analyte Recovery 2.6.2. Methodology 2.6.3. Recent ...
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... Extraction 3.6.1. Theoretical Considerations 3.6.2. Instrumentation 3.6.3 ... SOLIDS AND LIQUIDS Gregory C. Slack, Nicholas H. Snow, and Dawen Kou 4.1. 4.2 ... Solid-Phase Microextraction 155 156 158 159 161 163 163 164 170 170 173 173 ...
... Extraction 3.6.1. Theoretical Considerations 3.6.2. Instrumentation 3.6.3 ... SOLIDS AND LIQUIDS Gregory C. Slack, Nicholas H. Snow, and Dawen Kou 4.1. 4.2 ... Solid-Phase Microextraction 155 156 158 159 161 163 163 164 170 170 173 173 ...
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... Solid-Phase Extraction for Preconcentration Sample Preparation for Water Samples Precipitation Methods Preparation of Sample Slurries for Direct AAS Analysis Hydride Generation Methods Colorimetric Methods Metal Speciation 5.10.1. Types ...
... Solid-Phase Extraction for Preconcentration Sample Preparation for Water Samples Precipitation Methods Preparation of Sample Slurries for Direct AAS Analysis Hydride Generation Methods Colorimetric Methods Metal Speciation 5.10.1. Types ...
Page xiv
... Extraction and Precipitation 8.3.2. Membrane Filtration 8.4. Chromatographic Methods for the Purification of Nucleic Acids 8.4.1. Size-Exclusion Chromatography 8.4.2. Anion-Exchange Chromatography 8.4.3. Solid-Phase Extraction 8.4.4. A ...
... Extraction and Precipitation 8.3.2. Membrane Filtration 8.4. Chromatographic Methods for the Purification of Nucleic Acids 8.4.1. Size-Exclusion Chromatography 8.4.2. Anion-Exchange Chromatography 8.4.3. Solid-Phase Extraction 8.4.4. A ...
Contents
1 | |
SECTION A EXTRACTION AND ENRICHMENT IN SAMPLE PREPARATION | 37 |
CHAPTER 3 EXTRACTION OF SEMIVOLATILE ORGANIC COMPOUNDS FROM SOLID MATRICES | 139 |
CHAPTER 4 EXTRACTION OF VOLATILE ORGANIC COMPOUNDS FROM SOLIDS AND LIQUIDS | 183 |
CHAPTER 5 PREPARATION OF SAMPLES FOR METALS ANALYSIS | 227 |
SECTION B SAMPLE PREPARATION FOR NUCLEIC ACID ANALYSIS | 271 |
CHAPTER 7 SAMPLE PREPARATION IN RNA ANALYSIS | 301 |
CHAPTER 8 TECHNIQUES FOR THE EXTRACTION ISOLATION AND PURIFICATION OF NUCLEIC ACIDS | 331 |
SECTION C SAMPLE PREPARATION IN MICROSCOPY AND SPECTROSCOPY | 377 |
CHAPTER 10 SURFACE ENHANCEMENT BY SAMPLE AND SUBSTRATE PREPARATION TECHNIQUES IN RAMAN AND INFRARED SPEC... | 413 |
INDEX | 439 |
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Common terms and phrases
acid added addition allows amount Anal analysis analyte applications approach aqueous bonded bu¤er cell centrifugation Chem chemical chromatography coating column common complex compounds concentration containing depends described detection determined di¤erent digestion dissolved e¤ect electron elution ethanol example extraction fiber Figure followed groups headspace heating hydrophobic important increases injection interactions involves isolation layer less limit liquid materials matrix measurement membrane metals method minutes molecules needs obtained organic particles permission phase phenol plasmid polar possible precipitation present pressure procedure produce Raman range reaction recovery reduced referred relatively removed retained sample preparation selective separation shown silica soil solid solubility solution solvent sorbent species specimen SPME standard step surface Table techniques temperature tion tissue transfer trap tube typically vapor volatile volume
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