X-Ray Diffraction: A Practical ApproachIn this, the only book available to combine both theoretical and practical aspects of x-ray diffraction, the authors emphasize a "hands on" approach through experiments and examples based on actual laboratory data. Part I presents the basics of x-ray diffraction and explains its use in obtaining structural and chemical information. In Part II, eight experimental modules enable the students to gain an appreciation for what information can be obtained by x-ray diffraction and how to interpret it. Examples from all classes of materials -- metals, ceramics, semiconductors, and polymers -- are included. Diffraction patterns and Bragg angles are provided for students without diffractometers. 192 illustrations. |
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Contents
I | 3 |
II | 5 |
III | 14 |
IV | 18 |
V | 21 |
VI | 23 |
VII | 24 |
VIII | 27 |
XXV | 91 |
XXVI | 93 |
XXVII | 97 |
XXVIII | 125 |
XXIX | 153 |
XXX | 167 |
XXXI | 193 |
XXXII | 207 |
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Common terms and phrases
20 values alloy ångstrom body-centered cubic Bragg Bragg angle Bragg's law Bravais lattice broadening calculate the lattice components composition copper crystal structure crystallite Cu,Au cubic Bravais lattice determine diamond cubic diamond cubic structure diffraction peaks disordered electron energy equation example Experimental Module face-centered cubic fcc structure grain Hanawalt Search Manual hexagonal hkl a nm integrated intensity lattice parameter lattice parameter(s lattice point lattice strain measured metal Method Material Miller indices mixture NaCl nm Peak obtained ordered condition orthorhombic phase diagram planes positions Powder Diffraction radiation record the x-ray relative intensities shell shown in Fig silicon simple cubic sin² sin² 0 sin² sin² 0 values slits solid solubility solid solution ẞ phase structure factor Table Theta FIG Titanium two-phase unit cell unknown specimen wave wavelength x-ray diffraction pattern x-ray diffractometers x-ray photon