Characterization of Catalytic MaterialsCatalytic materials are essential to nearly every commercial and industrial chemical process in order to make reaction times faster and more efficient. Understanding the microstructure of such materials is essential to designing improved catalytic properties. This volume in the materials characterization series reviews the more common types characterization methods used for understanding surface and structural properties of most types of commercially used catalytic materials.
|
From inside the book
Results 6-10 of 40
Page 15
... studies of bulk metal catalysts, one may correlate the dynamics of surface chemical and physical changes with changes in the chemical and physical environment and thereby better understand the key principles govern- ing the catalytic ...
... studies of bulk metal catalysts, one may correlate the dynamics of surface chemical and physical changes with changes in the chemical and physical environment and thereby better understand the key principles govern- ing the catalytic ...
Page 17
... Studies of Supported Metals 2.4 X-ray Diffraction and Scattering Methods 2.5 Electron Microscopy 2.6 X-ray Absorption Spectroscopy 2.7 Mössbauer Spectroscopy 2.8 Photoelectron/Photoemission Spectroscopy 2.9 Magnetic Methods 2.10 Summary ...
... Studies of Supported Metals 2.4 X-ray Diffraction and Scattering Methods 2.5 Electron Microscopy 2.6 X-ray Absorption Spectroscopy 2.7 Mössbauer Spectroscopy 2.8 Photoelectron/Photoemission Spectroscopy 2.9 Magnetic Methods 2.10 Summary ...
Page 18
... studies have addressed the various definitions of particle size.1 The dispersion is the frac- tion of total metal that is actually exposed at a surface. The support can stabilize oxidation states that otherwise would not persist under ...
... studies have addressed the various definitions of particle size.1 The dispersion is the frac- tion of total metal that is actually exposed at a surface. The support can stabilize oxidation states that otherwise would not persist under ...
Page 19
... studies. X-ray absorption spectroscopy Variable Variable Variable Specifically suited for in situ studies. Table 2.1 Commonly applied probes of metals structure and catalyst environment condi- tions for their use. (The term “Variable ...
... studies. X-ray absorption spectroscopy Variable Variable Variable Specifically suited for in situ studies. Table 2.1 Commonly applied probes of metals structure and catalyst environment condi- tions for their use. (The term “Variable ...
Page 25
... Studies of catalysts based on measuring well-understood probe reactions comple- ment chemisorption studies in that both methods measure surface sites. Reaction studies of catalyst structures have the conspicuous advantage of providing ...
... Studies of catalysts based on measuring well-understood probe reactions comple- ment chemisorption studies in that both methods measure surface sites. Reaction studies of catalyst structures have the conspicuous advantage of providing ...
Contents
1 | |
17 | |
3 Bulk Metal Oxides | 47 |
4 Supported Metal Oxides | 69 |
5 Bulk Metal Sulfides | 89 |
6 Supported Metal Sulfides | 109 |
7 Zeolites and Molecular Sieves | 129 |
Methods of Preparation and Characterization | 149 |
LowEnergy Electron Diffraction LEED | 179 |
Mössbauer Spectroscopy | 180 |
Neutron Activation Analysis NAA | 181 |
Neutron Diffraction | 182 |
Physical and Chemical Adsorption for the Measurement of Solid Surface Areas | 183 |
Raman Spectroscopy | 184 |
Scanning Electron Microscopy SEM | 185 |
Scanning Transmission Electron Microscopy STEM | 186 |
Technique Summaries | 165 |
Auger Electron Spectroscopy AES | 167 |
Dynamic Secondary Ion Mass Spectrometry DSIMS | 168 |
Electron Energyloss Spectroscopy in the Transmission Electron Microscope EELS | 169 |
Electron Paramagnetic Resonance Electron Spin Resonance | 170 |
Electron Microprobe XRay Microanalysis EPMA | 171 |
EnergyDispersive XRay Spectroscopy EDS | 172 |
Extended XRay Absorption Fine Structure EXAFS | 173 |
Fourier Transform Infrared Spectroscopy FTIR | 174 |
High Resolution Electron Energy Loss Spectroscopy HREELS | 175 |
Inductively Coupled Plasma Mass Spectrometry ICPMS | 176 |
Inductively Coupled PlasmaOptical Emission Spectroscopy ICPOES | 177 |
Ion Scattering Spectroscopy ISS | 178 |
Scanning Tunneling Microscopy and Scanning Force Microscopy STM and SFM | 187 |
Solid State Nuclear Magnetic Resonance NMR | 188 |
Static Secondary Ion Mass Spectrometry Static SIMS | 189 |
Temperature Programmed Techniques | 190 |
Transmission Electron Microscopy TEM | 191 |
Ultraviolet Photoelectron Spectroscopy UPS | 192 |
XRay Diffraction XRD | 193 |
XRay Fluorescence XRF | 194 |
XRay Photoelectron and Auger Electron Diffraction XRD and AED | 195 |
XRay Photoelectron Spectroscopy XPS | 196 |
Index | 197 |
Other editions - View all
Common terms and phrases
acid adsorbed adsorption alloys alumina aluminum analysis atoms beam bond bulk metal calcination Catal catalytic activity catalytic behavior catalytic materials cation Chem chemical chemical shifts chemisorption Chemistry cobalt coordination crystalline crystallites desorption determine electron microscopy elements energy EXAFS faujasites Figure function hydrogen hydrogenolysis I. E. Wachs interaction lattice layer measured metal catalysts metal oxide catalysts metal oxide overlayers metal oxide phases microporous Mo ions molecular sieves molecules molybdenum oxide monolayer coverage MoS2 Mössbauer Mössbauer spectroscopy neutron obtained oxide support oxygen particle peak photoelectron pillared clays pore powder preparation probe promoter R. R. Chianelli Raman Raman spectroscopy reaction reduced resolution ruthenium sample single crystal solid solution species spectra spectroscopy structure studies sulfides sulfur supported metal oxide surface area surface metal oxide synchrotron techniques temperature temperature-programmed thiophene tion transmission electron microscopy two-dimensional metal oxide X-ray absorption X-ray diffraction XANES zeolites